Tbaf Nmp Etchant

TBAF/NMP etchant is a solution of tetrabutylammonium fluoride (TBAF) in N-methyl-2-pyrrolidone (NMP) used to remove silicon oxide and other fluoride-reactive materials in micro- and nanofabrication. The fluoride ions attack silicon-oxygen bonds, converting oxide components into soluble fluorinated species, while the polar aprotic NMP solvent helps maintain a workable, nonaqueous etching environment. Engineers use this etchant for surface cleaning, oxide pattern transfer, sacrificial-layer removal, and selective preparation of silicon-based devices. Its compatibility with nonaqueous processing makes it useful when controlled oxide removal is needed near moisture-sensitive materials or structures.

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Education

JoVE Science Education - Chemistry

Nuclear Magnetic Resonance (NMR) Spectroscopy

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2023

Source: Laboratory of Dr. Henrik Sundén – Chalmers University of Technology Nuclear magnetic resonance (NMR) spectroscopy is a vital analysis technique for organic chemists. With the help of NMR, the work in the organic lab has been facilitated tremendously. Not only can it provide information about the structure of a molecule but also determine the content and purity of a sample. Compared with other commonly encountered techniques for organic chemists — such as thermal analysis and mass...

Research

JoVE Journal - Chemistry

Application and Methodology of the Non-destructive 19F Time-domain NMR Technique to Measure the Content in Fluorine-containing Drug Products

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Cited by 2 •

2017

A simple and non-destructive technique that measures the average content of drug substances in formulated drug products containing fluorine using low-field fluorine-19 (19F) time-domain (TD) nuclear magnetic resonance (NMR) is presented here. The technique can be applied to the development and manufacturing of drugs in the pharmaceutical industry.

Hyperpolarized Xenon for NMR and MRI Applications

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Cited by 28 •

2012

The production of hyperpolarized xenon by means of spin exchange optical pumping (SEOP) is described. This method yields a ~10000-fold enhancement of the nuclear spin polarization of Xe-129 and has applications in nuclear magnetic resonance spectroscopy and imaging. Examples of gas phase and solution state experiments are given.

Electrochemical Etching and Characterization of Sharp Field Emission Points for Electron Impact Ionization

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2016

A method for electrochemically etching field emission tips is presented. Etching parameters are characterized and the operation of the tips in field emission mode is investigated.

Research

JoVE Journal - Chemistry
Free Sample

Spin Saturation Transfer Difference NMR (SSTD NMR): A New Tool to Obtain Kinetic Parameters of Chemical Exchange Processes

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Cited by 4 •

2016

A detailed protocol describing the SSTD NMR method is presented here to help new users apply this new method to obtain the kinetic parameters of their own systems undergoing chemical exchange.

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