<p class="jove_content">This protocol presents an operando electrochemical XPS platform for aqueous electrocatalysis, enabling catalyst characterization during membrane-electrode-assembly water electrolysis and three-electrode measurements. It combines controlled electrolyte delivery, Au-grid electrical contact, near-ambient-pressure XPS, optional gas/QMS analysis, and temperature control to study catalyst transformations under operating conditions.</p>

design-operation-versatile-operando-electrochemical-x-ray

Design and Operation of a Versatile Operando Electrochemical X-ray Photoelectron Spectroscopy Platform for Aqueous Electrocatalysis

Understanding electrocatalyst activation and degradation under realistic operating conditions requires operando spectroscopic techniques capable of ...

Institution - Univ. Savoie Mont Blanc, CNRS, Grenoble INP, LEPMI

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